TY - JOUR AU - Samedinov, Maksut AU - Arslan, Gulsin AU - Sargin, Idris PY - 2026 DA - 2026/08/04 TI - Enhanced Degradation of Methylene Blue and Methyl Orange Dyes Using Fe<sub>3</sub>O<sub>4</sub>@N-MWCNT as a Peroxymonosulfate Activator JO - Catalysis Research SP - 009 VL - 06 IS - 03 AB - Peroxymonosulfate decomposition is crucial for environmental remediation, especially in degrading organic pollutants. Peroxymonosulfate can be oxidized by transition metals, generating hydroxyl and sulfate radicals that degrade pollutants. In this study, a heterogeneous catalyst (Fe3O4@N-MWCNT, a composite of Fe3O4 with nitrogen-doped multi-walled carbon nanotubes) was prepared, characterized (FT-IR, TEM, XRD, DSC), and used as a peroxymonosulfate activator for the degradation of Methylene Blue and Methyl Orange dyes in aqueous media. The results indicated that Fe3O4@N-MWCNT could serve as an effective peroxymonosulfate activator, reducing degradation times from hours to seconds (Methylene Blue: >180 min. to 32 s; Methyl Orange: >20 min. to 6 s). Moreover, the Fe3O4@N-MWCNT catalyst maintained its activity over 5 cycles. This study demonstrated that Fe3O4@N-MWCNT can serve as a highly effective activator of peroxymonosulfate, thereby holding significant potential for remediating water sources contaminated with Methylene Blue and Methyl Orange dyes. SN - 2771-490X UR - https://doi.org/10.21926/cr.2603009 DO - 10.21926/cr.2603009 ID - Samedinov2026 ER -